With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.14871-92-2,(2,2¡ä-Bipyridine)dichloropalladium(II),as a common compound, the synthetic route is as follows.
General procedure: To a vigorously stirred solution of BzpheH2 (32.32 mg, 0.12 mmol) in 8 mL CH3OH/H2O (V:V 1:1), [Pd(bipy)Cl2] (20 mg, 0.06 mmol) was added. The mixture was heated to 50C and adjusted to pH 8-9 by NaOH solution, and then stirred for 2 h. The solution was concentrated to about 80% of the original volume. The complex I-a was separated from the solution after a few days.
The synthetic route of 14871-92-2 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Wang, Li-Wei; Liu, Si-Yuan; Wang, Jin-Jie; Peng, Wen; Li, Sheng-Hui; Zhou, Guo-Qiang; Qin, Xin-Ying; Wang, Shu-Xiang; Zhang, Jin-Chao; Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry; vol. 45; 7; (2015); p. 1049 – 1056;,
Chapter 1 An introduction to palladium catalysis
Palladium/carbon catalyst regeneration and mechanical application method