Awesome and Easy Science Experiments about Tetrakis(acetonitrile)palladium(II) tetrafluoroborate

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The simple synthetic conversion of a 90-angled bis-pyridyl ligand into a tripodal tris-pyridyl ligand leads to the formal transformation of a cubic (a=b=c) into a square-cuboid (a=b?c) coordination cage. Mathematical considerations associated with the ligand design, together with X-ray structure results, NMR spectroscopic and mass spectrometric characterization and molecular modeling of both coordination cages are presented and discussed. Minecraft with molecules: The simple synthetic conversion of a 90-angled bis-pyridyl ligand into a tripodal tris-pyridyl ligand leads to the formal transformation of a cubic (a=b=c) into a square-cuboid (a=b?c) coordination cage. The ligand design based on mathematical considerations, X-ray structure results, NMR spectroscopic and mass spectrometric characterization and molecular modeling of both coordination cages are presented.

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Reference:
Chapter 1 An introduction to palladium catalysis,
Palladium/carbon catalyst regeneration and mechanical application method