Discovery of (2,2′-Bipyridine)dichloropalladium(II)

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One of the major reasons for studying chemical kinetics is to use measurements of the macroscopic properties of a system, HPLC of Formula: C10H8Cl2N2Pd, such as the rate of change in the concentration of reactants or products with time.In a article, mentioned the application of 14871-92-2, Name is (2,2′-Bipyridine)dichloropalladium(II), molecular formula is C10H8Cl2N2Pd

The results of an investigation on catalytic systems arising from the electrochemical activation of salts and complexes of several transition metals for the carbonylation of methanol to dimethylcarbonate (DMC) are reported. Metals were tested as inorganic salts or complexes with ligands such as 2,2?-bipyridine (bipy), 1,6-bis (2-oxyphenyl)-2,5-diaza-1,5-hexadiene (salen), 2,4-pentanedionate (acac), triphenylphosphine (TPP) in methanol at room temperature saturated with carbon monoxide at atmospheric pressure. Best faradic yields vs DMC were observed as follows: CuCl(bipy): 84.8%; PdCl2(bipy): 64.0%; CoCl2: 26.0%; RhCl3: 25.0%; AgBF4(bipy): 10.2%; AuCl3: 9.4%; Cr(acac)3: 6.7%; PtCl2(bipy): 2.1%; NiCl2: 1.8%. The influence of the ligand on faradic yields has been also investigated.

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Reference：
Chapter 1 An introduction to palladium catalysis,
Palladium/carbon catalyst regeneration and mechanical application method