Discovery of Bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II)

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Bifurans via palladium-catalyzed Suzuki coupling

Sixteen 2,2′-bifurans with aryl substituents are reported. The copper-mediated oxidative coupling of lithium salt of furan led to the formation of 2,2′-bifuran, which was brominated with either 2 eq. or 4 eq. NBS to afford 5,5′-dibromo-2,2′-bifuran and 3,3′,5,5′-tetrabromo-2,2′-bifuran. The palladiumcatalyzed Suzuki reactions between dibromo or tetrabormo-bifuran and arylboronic acid were employed to furnish the title compounds, which were characterized by NMR spectra and mass spectra.

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Reference£º
Chapter 1 An introduction to palladium catalysis,
Palladium/carbon catalyst regeneration and mechanical application method