(2,2¡ä-Bipyridine)dichloropalladium(II), cas is 14871-92-2, it is a common heterocyclic compound, the catalyst-palladium compound, its synthesis route is as follows.
(bpy)PdCl2 (167 mg, 0.5 mmol) and AgNO3 (170 mg, 1.0 mmol) was mixed in CH3NO2 (40 mL). The mixture was stirred at 60 C for 24 hrs, and the white AgCl precipitate was filtered by a short pad of celite. The filtrate was sampled for ESI-HRMS, and cationic C20H18N4O2Pd22+ (m/z: 279.9743) was observed. Then the filtrate was concentrated and recrystallized to give 25 mg light yellow needle-like solid. Yield 9.0%.
14871-92-2 is used more and more widely, we look forward to future research findings about (2,2¡ä-Bipyridine)dichloropalladium(II)
Reference£º
Article; Yang, Zhenyu; Ni, Yuxin; Liu, Rui; Song, Kaixuan; Lin, Shaohui; Pan, Qinmin; Tetrahedron Letters; vol. 58; 21; (2017); p. 2034 – 2037;,
Chapter 1 An introduction to palladium catalysis
Palladium/carbon catalyst regeneration and mechanical application method